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Bioepoxy/Clay Nanocomposites: Fabrication Optimisation, Properties and Modelling
Haipan Salam
(Author)
·
Yu Dong
(Author)
·
Springer
· Paperback
Bioepoxy/Clay Nanocomposites: Fabrication Optimisation, Properties and Modelling - Salam, Haipan ; Dong, Yu
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Synopsis "Bioepoxy/Clay Nanocomposites: Fabrication Optimisation, Properties and Modelling"
Chapter 1. Introduction1.1. Biopolymers1.5.1. Renewable polymers1.5.2. Petroleum-based biopolymers1.5.3. Biopolymers from mixed sources1.2. Nanofillers1.2.1. Nanoclay fillers1.2.1.1. Montmorillonite (MMT) nanoclays1.2.1.2. Halloysite nanotubes (HNTs)1.2.1.3. Immogolite nanotubes (INTs)1.2.2. Nanoclay modification1.2.3. Nanoclay dispersion status1.3. Fabrication of biopolymer/clay nanocomposites1.4. Optimization technique and effective synthesis1.5. Nanocomposite properties1.5.1. Mechanical properties1.5.2. Thermal properties1.5.3. Biodegradability1.5.4. Barrier properties and water absorptionChapter 2 Experimental design, fabrication and characterization techniques2.1. Design of Experiments (DoEs)2.1.1. Taguchi method2.1.2. Pareto analysis of variance (ANOVA)2.1.3. Confirmation tests2.2. Fabrication of bioepoxy/clay nanocomposites2.3. Experimental characterization2.3.1. Morphological structure analysis2.3.1.1. X-ray diffraction (XRD) analysis2.3.1.2. Transmission electron microscopy (TEM)2.3.1.3. Scanning electron microscopy (SEM)2.3.1.4. Fourier transform infrared (FTIR) analysis2.3.2. Mechanical testing2.3.2.1. Tensile testing2.3.2.2. Flexural testing2.3.2.3. Charpy impact testing2.3.2.4. Durometer hardness testing2.3.3. Differential scanning calorimetry (DSC)2.3.4. Composting tests2.3.5. Water absorptionChapter 3 Optimization of material formulation and processing parameters of bioepoxy/clay nanocomposites3.1. Mechanical properties of bioepoxy/clay nanocomposites based on Taguchi DoEs3.2. Evaluation of significant factors3.3. Preferred combination factors3.4. Confirmation tests3.5. Structure-property relationshipChapter 4 Morphological structures of bioepoxy/clay nanocomposites with optimum formulation4.1. FTIR spectra4.2. XRD patterns4.2.1. Effect of clay content4.2.2. Effect of epoxidized soybean oil (ESO) content4.3. TEM observation4.4. SEM morphologyChapter 5 Material properties of bioepoxy/clay nanocomposites with optimum formulation5.1. Mechanical properties5.2. Thermal properties5.3. Biodegradation properties5.3.1. Water absorption5.3.2. BiodegradabilityChapter 6 Theoretical modeling of bioepoxy/clay nanocomposites6.1. Theoretical models6.1.1 Modulus of polymer particulate composites6.1.1.1 Rule of mixture (ROM)6.1.1.2 Modified rule of mixture (MROM)6.1.1.3 Hirsch model6.1.1.4 Halpin-Tsai model6.1.1.5 Hui-Shia model6.1.1.6 Laminate model6.1.2. Strength of polymer particulate composites6.1.2.1 Danusso-Tieghi (D-T) model6.1.2.2 Nicolais-Narkis (N-N) model6.1.2.3 Lu model6.1.2.4 Turcsányi-Pukànszky-Tüdõs (T-P-T) model6.2. Estimation on tensile modulus of bioepoxy/clay nanocomposites6.2.1. The effect of clay content6.2.2. The effect of ESO content6.3. Estimation of tensile strength of bioepoxy/clay nanocomposites6.3.1. The effect of clay content6.3.2. The effect of ESO contentChapter 7 Nanocomposite applications7.1. Automotive applications7.2. Material packaging applications7.3. Medical applicationsReferencesAppendices
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